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Welcome to Organic Chemistry 360’s Laboratory Report Workbook
This Report Book, along with the ‘Chemistry 360 Lab Manual’, will help you prepare for four-five days straight of supervised lab instruction. All preparatory work in this report book (~12 h to finish, see list on page 3), may be completed and shown to the Chemistry Lab Co-ordinator / Lab Instructor prior tobeginning the labs.In order to successfully complete the laboratory component, please be aware of the following 4 step process of instruction. It is the intention of this Chem360 Report Workbook to provide you with the means of completing all four steps.
Step 1: First we tell you what you are going to do.
Find out by reading the lab manual, doing the pre-lab questions in this report book, and filling out the Table of Reagents etc., i.e., preparing for the labs at home.(By doing so you are able to work more efficiently in the lab and the over-all time spent in the supervised lab can be the usual 32 hours.)
Step 2: Next we show you how to do it.
When you come to the lab, a lab instructor will give a safety orientation, followed by a series of mini lab lectures on each experiment. Various techniques will be demonstrated and you will be shown how to handle chemicals, dispose of hazardous waste, and operate the equipment
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How to best do the Report Book Exercises
1. First read through the lab manual introduction, and then answer the pre-lab questions for each experiment.
2. Complete the Objectives in the Experiment Report.
3. Complete the Procedure (Refer to lab manual pages) and make a flowchart if necessary.
4. Complete the Table of Reagents for each experiment (detach a copy of the TOR to avoid flipping back and fort
ExperimentPost Lab Questions:
1. If the cost of both the alcohol and carboxylic acid were prohibitive, how would you maximize the yield of your Fischer esterification product while keeping costs down?
2. Why did you wash your product with water (3X), before washing it with the solution of sodium hydrogen carbonate? What was the purpose of washing with sodium hydrogen carbonate?
3. Explain the function of the acid catalyst in a Fisher esterification reaction.
4. What would the reactants be to produce isoamyl valerate via Fischer esterification reaction.
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